Solid Phase Extraction Chromatography PowerPoint PPT Presentations

... Procedure for Using Maxi-Clean IC Cartridges. 1. Precondition the cartridge by passing 5-10mL of IC grade ... Precondition IC-Na cartridge with 5mL water. 2. ...

DISPLACEMENT EFFECTS IN SPE OF PEPTIDES: [Ovalbumin Peptide Mix] Selectivity of Adsorption Removal of 1 M Urea from a Tryptic Digest

Making MI polymers Polymerization Reaction components ... Journal of Pharmaceutical and Biomedical ... Synthesis and Application of Molecularly Imprinted Solid ...

Title: No Slide Title Author: RPP WTP Last modified by: Meg Mercer Created Date: 3/12/2003 11:35:00 PM Document presentation format: On-screen Show

He invented this technique to 'address the need for a fast, solvent-free, and ... a dual o-ring that creats a hermetic seal to preserve and protect SPME holder/sample. ...

Lecture 7 Chromatography Intro! Lecture 7 Chromatography Intro! Compounds of interest stick to sorbent Solid Phase Extraction Load (sample) Compounds of interest ...

Volatile organic compounds (VOCs) are found throughout our environment and can ... Hewlett Packard 5890A Chromatograph with an FID ...

Supercritical fluid methods Ji Kone n 2005 Sample is solid phase CFE - Supercritical fluid extraction SFC - Supercritical fluid chromatography Why use ...

Gas Chromatography Introduction 1.) Gas Chromatography Mobile phase (carrier gas) is a gas Usually N2, He, Ar and maybe H2 Mobile phase in liquid chromatography is a ...

The retardation factor (Rf) can be calculated to quantify the distance traveled by a compound. Thin Layer Chromatography TLC is only qualitative, not quantitative.

1903 Tswett - plant pigments separated on chalk columns (radial chromatography) ... each component of the mixture, and many cycles of this process during elution ...

Hair A valuable resource in post-mortem toxicology ... Drugs were extracted from the hair samples using 0.1 M HCl followed by solid phase extraction clean-up.

Title: High Performance Liquid Chromatography Author: ITC Labs & Classrooms Last modified by: Vaughn C. Kowahl Created Date: 4/1/1998 12:50:26 AM Document ...

Gas Chromatography (GC) Instruments for gas-liquid chromatography 1- Carrier gas supply 2- Sample injection system 3- Column configuration and column ovens 4 ...

Part 2: Case studies Dr. C.B. Perry (C306) http://www.gh.wits.ac.za/chemnotes Chem 3033 Extraction Metallurgy Gangue pronounced gang dump leaching, relatively ...

GAS CHROMATOGRAPHY CHAPTER 21 Gas Chromatography Produces Chromatograms GC is used to identify, (compare to standards) separate, and quantify (use peak area) samples.

It deals in detail concept of thin layer chromatography (TLC)

Flowing mobile phase (inert gas - Ar, Ne, N) Injection port ( rubber septum ... Cocaine in Fruit Flies: A Study of Neurotransmission by Prof. Jay Hirsh, UVa ...

PLANNAR CHROMATOGRAPHY It includes two types: 1- Thin Layer Chromatography (TLC). 2- Paper Chromatography (PC). Thin Layer Chromatography (TLC) In this type a thin ...

In gas chromatography, vapor-phase analyte is swept through the column by a ... The trap contains particles made of adsorbent compounds that the analytes adsorb onto. ...

A gas or liquid mixture carrying several components is passed as a mobile ... Diatomaceous earth impregnated with ethylene glycol (old method, poor selectivity) ...

Sensitive to halogen-containing and other electronegative compounds. Based on the capture of electrons by electronegative atoms ...

Introduction to chromatography tecniques

What is Chromatography? Chromatography is a physico chemical process that belongs to fractionation methods same as distillation, crystallization or fractionated ...

Eluent Strength. Strong mobile phase compositions make solute elute faster. ... polar mobile phases have higher eluent strength. Reversed Phase ...

Chapter 21 Principles of Chromatography * * * * * * 21-3 Why do bands spread ? 6) Plate height equation Plate height equation 21-3 Why do bands spread ?

V2 = volume of solvent 2 (extraction solvent) Extraction is a power function. 3 ... Gel Permeation. Similar to HPLC. 9. Immobilized Antibody Separation. 10 ...

Theory Instrumentation Properties of supercritical fluid Critical temperature Above temperature liquid cannot exist Vapor pressure at critical temperature is critical ...

Title: Lecture note : Gas chromatography [1] Subject: GC, carrier gas, inlet, column, , , Author

Introduction Solvents & Reagent Quality Mobile phase preparation & usage Buffer, Filtration, Degassing Storage & usage Preparation for analysis Sample preparation & System suitability Resolution, peak symmetry, tailing, capacity factor, Adjustment allowed as per USP Column management Washing and change of mobile phase Analysis and integration Audit trail, data backup, Review and Documentation Problems and reporting Qualification and Calibration

A Photoionization Reaction If the amount of ionization is reproducible for a given compound, pressure, ... (like organosulfur or organophosphorus species) ...

The five gases commonly used as carrier gas and detector fuels in capillary gas chromatography are helium ... Hot flash vaporization Direct ...

page 675 http://en.wikipedia.org/wiki/Mikhail_Tsvet The method was described on 30 December 1901 at the XI Congress of Naturalists and Physicians (XI ...

Detectors of a gas chromatograph Kovat Retention Index Isothermal I = 100n + 100[(log t R(x) log t R(n)) / (log t R(n+1)-log t R(n))] I = retention index ...

Chapter 4 High Performance Liquid Chromatography HPLC 1952 A.J.Martin and R.L.M.Synge received the Nobel Prize for the discovery of ...

The distillation of liquids that are fully miscible is governed by Raoult's Law ... The mixture will have its own unique boiling point ... 'gnosis' or knowledge. ...

, Supercritical Fluid Extraction, Chromatography and Other Applications

High pressure liquid chromatography High priced ... Biomedical and Clinical HPLC applications include detection, ... APPLICATIONS OF HPLC Slide 30 ...

Chromatographic Separation and Measurement of Charged-Particle Emitting Radionuclides ... Ludwick, Health Physics, 1961, 6, 63-65. ...

Thin Layer Chromatography: 'The separation of moderately volatile or ... 'Analgesia': Greek for the deadening or absence of pain without loss of consciousness ...

Cotinine eluted using salt gradient onto analytical column. Chromatogram. A ... phenomenon caused by compounds that co-elute with the compound of interest and ...

* * * Matter Mixtures Pure substances Homogeneous Heterogeneous Compounds ... Chromatography of plant pigments Extraction: ... Waste: Liquid Waste should go in ...

Anionic exchanger: positively charged functional groups and exchanges ... Negatively charged molecules attracted to DEAE-cellulose (the anionic exchanger) ...

none

Chemical Separation is a central part of analytical chemistry. Analytical chemistry: What? ... (CEC) Reversed- phase. Capillary. Electro- chromatography ...

The biggest reason for continued interest in Chemical Diversity is the recent ... Resins as isopycnic slurries. Purification Methods. Solid Phase. Wash exhaustively ...

a process whereby the compounds of. interest are removed from ... Lyophilization. 10. Extraction. sample. liquid. solid. liquid. to. liquid. Liquid to. liquid ...

GLACEO Workshop October 15-17, 2004 Sensors, Instruments and Tools Comprehensive 2-Dimensional Gas Chromatography Coupled with Time-of-Flight Mass Spectrometry

Analysis of Botanical Dietary Supplement Ingredients for Pesticides using QuEChERS Combined with Capillary Gas Chromatography-Triple Quadrupole Mass Spectrometry:

Chapter 24 GC Gas Chromatography

Dong-Sun Lee/ CAT-Lab / SWU Chapter 33 Supercritical Fluid Chromatography Supercritical Fluid Chromatography (SFC) In supercritical fluid chromatography (SCF) the ...

Bitter tasting, generally white solids (exception - nicotine is a brown liquid) ... Physical & chemical properties. ???????? ????? ??? ??????????? ?????. ?????? ...

As mixture begins to boil, the vapor phase becomes richer in A than the liquid phase! ... Ethanol is the more volatile material (it will boil first) ...

max wellington id# ud3587sch8551 course: instrumental methods : chromatography topic: gas chromatography and its use in the determination of oxalates in bayer process ...

Ball Mill: solid. Frozen cell paste, cells attached to or within a solid matrix. Large scale ... To pump a slurry (up to 1500 bar) through a restricted orifice valve. ...

Soxhlet. d. Supercritical fluid extraction. e. Sublimation. f. Steam distillation. Fractionation Isolation 1. Hydrophobicity or hydrophilicity 2.