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Electron Microprobe Laboratory Other titles: Times New Roman Arial Default Design Slide 1 ... – PowerPoint PPT presentation

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Title: sample


1
1. Free electrons are created in the Electron
Gun by heating a tungsten filament (Cathode)
2. Electrons are accelerated down the electron
optical column by means of a high voltage
potential at the Anode
Energy Dispersive X-ray Analyzer
3. The electron flux is shaped into a beam by
the Condenser Lenses
x-rays resolved on the basis of their energies
4. The beam current is controlled by the Beam
Regulation Aperture (and the condenser lenses)
5. The beam current is measured with, or
permitted down the column by removing, the
Faraday Cup
6. Beam ellipticity is corrected by the Stigmator
7. The beam is scanned or fixed into a probe
spot by the Final Condensing (objective) Lens
diffraction crystal
8. The beam impacts the sample, giving rise to
various signals including secondary electrons,
backscattered electrons, x-rays, and
cathodoluminescent energy. Current absorbed by
the sample also can be imaged.
x-rays
Secondary Electron Detector
detects low-energy electrons liberated from near
the sample surface, providing an image of sample
topography
sample
scintillation counter
Backscattered Electron Detector
detects higher-energy electrons bounced out of
the sample, providing an image based on average
atomic mass (related to density) hence, the
image is based on the compositions of constituent
components
Wavelength Dispersive Spectrometer
x-rays resolved by diffraction, through a regular
periodic solid, to a gas-filled counter
Absorbed CurrentMeter
images electrical conductivity within the sample
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