surface area and pore size distribution analyser by static volumetric principle - PowerPoint PPT Presentation

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surface area and pore size distribution analyser by static volumetric principle

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Gold APP Instruments () Corporation China is a high-tech company specialized in laboratory and analytical instruments making, such as BET surface area analyzer, surface area and pore size analyzer, gas pycnometer helium true density analyzer, high pressure and high temperature gas sorption analyzer, sample preparation degasser and so on for particle, porous, powder and fiber materials by measuring methods BET surface method, Langmuir surface, t-plot, BJH pore size, pore volume, pore size distribution, MP micropore, SF, HK, DR, DA micropore and mesopore analyzing. Web: Tel.: 0086-18210009838 Skype: Gold-APP-Instruments Yahoo Messenger: goldappinstruments@ymail.com Gtalk: goldappinstruments2008@gmail.com – PowerPoint PPT presentation

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Title: surface area and pore size distribution analyser by static volumetric principle


1
Gold APP Instruments
  • Leader in
  • BET surface area analyzers
  • Surface area and pore size distribution analyzers
  • Gas pycnometer true density analyzers
  • High pressure gas sorption analyzers
  • Sample degassers

2
V-Sorb 2800 surface area and porosimetry
analyzer introduction
3
V-Sorb 2800surface area and porosimetry analyzer
introduction
  • V-Sorb 2800 is researched by Gold APP
    Instruments for surface area and pore
    size testing by utilizing static volumetric
    principle. Compared with other competitors
    analyzers, multi pioneered technologies make its
    performance much better. Heighten accuracy and
    consistence of results, enhance measurement
    stability, all these lead to a leading
    level among global competitors. Equipment
    designed from the user perspective and with fully
    automated operation system, user-friendly
    interface makes it easy to learn, imported
    accessories assure stability and prolong
    its life.

4
V-Sorb 2800 surface area and porosimetry
analyzer parameters- Part 1
  • Analysis Method static volumetric nitrogen
    adsorption principle
  • Versatility Adsorption and desorption isotherms,
    Single and multi-point BET surface area, Langmuir
    method surface area, Average particle diameter
    estimation, t-plot external surface area, True
    density analysis, BJH total pore volume and pore
    size distribution analysis, t-plot method
    micropore analysis, MP micropore,
    Dubinin-Radushkevich (DR) and Dubinin-Astakhov
    (DA) micropore surface area
  • Measuring Ranges 0.01m2/g to no known upper
    limit (surface area)
  • 0.35 to 400nm
    (pore size)
  • Vacuum System V-Sorb unique monolithic manifolds
    and electromagnetically operated valve control
    system, greatly reduce the dead volume improve
    the adsorbate micro-change sensitivity enhance
    pore size distribution analysis resolution
    decrease connecting points strengthen sealing
    performance and prolonged instrument life

5
V-Sorb 2800 surface area and porosimetry
analyzer parameters- Part 2
  • Accuracy repeatability errors 1
  • Coolant Level Prober V-Sorb original coolant
    level probe system with temperature probe, ensure
    the coolant level unchanged when compares with
    sample cells in the whole analysis process,
    completely eliminate the analysis errors caused
    by dead volume change
  • Sample Treatment the whole treatment procedures
    are controlled by dedicated software, as well
    with a start time preset function which can
    realize unattended operation at night
  • Control System programmable controller
    electromagnetically operated valve system with
    high integration and strong anti-interference
    ability, enhance instruments stability and life
  • Sample Ports2 samples analyzing and 2 samples
    degassing concurrently

6
V-Sorb 2800 surface area and porosimetry
analyzer parameters- Part 3
  • Pressure Measurement imported sectional
    measuring dual pressure transducer, notably
    improve the measuring accuracy at low P/Po point,
    0-1000Torr (0-133Kpa), 0-10Torr (0-1.33Kpa)
  • Transducer Accuracy imported silicon thin film
    pressure transducer, accuracy can reach 0.1 of
    real reading, better than 0.1 of
    F.S.(full-scale), far accurate than Pirani
    resistance vacuum gauge(general error is 10-15)
  • Partial Pressure P/Po controllable accuracy
    range is 5x10-6-0.995
  • Ultimate Vacuum 4x10-2Pa (3x10-4Torr)
  • Sample Types powders, particle, fiber, flakes
    and other species
  • Adsorbate Gas high purity nitrogen (99.999),
    Ar, Kr, CO, CO2, C4H10 etc. non-corrosive gases
    are optional
  • Data Acquisition high-precision and high
    integration data acquisition modules, minimal
    error, strong anti-interference ability
  • Data Reduction Windows-based independent
    developed Gold APP softwareTM, perfect
    versatility, produced full featured and
    multi-model reports

7
V-Sorb 2800 surface area and porosimetry
analyzer features-Part 1
  • A Vacuum System
  • 1. Unique integral manifolds system, decrease
    connecting points apparently, reduce leak rate,
    improve ultimate vacuum.
  • 2. Modularity design can configure as customer
    requests, benefits future functions extension and
    instrument maintenance.
  • 3. Germany imported bipolar vacuum pump, low
    noise, stable working, oil-return prevention
    ultimate vacuum can reach 4x10-2Pa (3x10-4Torr).
  •  
  • B Control System
  • 1. Industry used programmable controller
    electromagnetically operated valve system, strong
    anti-interference ability, convenient for
    installation and uninstallation.
  • 2. Separated analysis and treatment manifolds can
    prevent foreign matter to contaminate manifolds
    in sample treatment.

8
V-Sorb 2800 surface area and porosimetry
analyzer features-Part 2
  • C. Measures for Improving Accuracy
  • 1. Imported silicon thin film capacitive pressure
    transducer, accuracy can reach 0.1 of real
    reading, better than 0.1 of F.S. (full-scale).
  • 2. 0-10Torr (optional) and 0-1000Torr dual
    transducers, sectional measurement in pressure
    range can reduce errors in low vacuum, 0-10Torr
    silicon thin film transducer is highly accurate
    than Pirani resistance vacuum gauge (general
    error is 10-15).
  • 3. Unique monolithic manifolds system, decrease
    connecting points and reduce leak rate
    apparently.
  • 4. Original stepping coolant level control
    system, ensure the coolant level unchanged when
    compares with sample cells in the whole analysis
    process, completely eliminate the analysis errors
    caused by dead volume change.
  • 5. Pioneered gas outlet and inlet control system
    can efficiently prevent sample splash in
    evacuation and gas inlet process, guarantee clean
    manifolds and sample weight unchanged, avoid zero
    and liner drifting caused by transducers
    macro-change.

9
V-Sorb 2800 surface area and porosimetry
analyzer features-Part 3
  • D. Data Acquisition and Reduction
  • 1. High precision and integration data
    acquisition module is easy to connect, minimal
    errors and strong anti-interference ability
    standard 485 communication mode is good for
    analyzers applications extension and
    interconnection, can also conveniently switched
    to RS232 and USB modes.
  • 2. Multi calculating methods for data reduction
    provides all-round sample analysis options
    powerful data archiving and searching system
    helps a lot for data management.

10
V-Sorb 2800 surface area and porosimetry
analyzer application
  • 1. Super micro powder, nanomaterials, particle
    and fiber shaped surface area analysis.
  • 2. Product quality control for powder species
    related corporations.
  • 3. Research institutes, universities for BET
    theory teaching.
  • 4. Full cells, catalysts, additives, adsorbent,
    ceramics, magnetic materials, energy storage
    materials etc.
  • 5. Other researches concern surface area
    performance.

11
Gold APP Instruments
  • Webs www.jinaipu.com
  • www.app-one.com.cn
  • Email sales_at_jinaipu.com
  • goldapp_at_msn.com
  • Tel 86-18210009838
  • Fax 86-10-82118197
  • Skype Gold-APP-Instruments
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